Posts by Ghost

Seriously thanks for shitting up my thread with your fucking retardation

You want to fuck with my threads with your stupid bullshit posts? Fucking bitch I can play the same game.

2018-06-17 at 10:18 PM UTC in Unban Wellhung

Ghost Black Hole

I don't remember "Being a Cunt" being against the rules.

Lanny is guilty of that every day of his life lol so he should permanently ban himself

(Pics of a REAL forum I used to run where nobody ever got banned)

2018-06-17 at 10:15 PM UTC in are you friends with your neighbors?

Ghost Black Hole

I dont have any IRL friends :(

2018-06-17 at 10:10 PM UTC in Unban Infinityshock

Ghost Black Hole

I was a mod on hell (it is a forum) and we never had problems with any users because our mod/admin team just didn't give a fuck.

https://steamcommunity.com/groups/oddwebsite

The forum

2018-06-17 at 10:06 PM UTC in Dhers...Remember The Fun Times, Too Bad NISers

Ghost Black Hole

Join the anti DH KKK!

https://niggasin.space/thread/25442

2018-06-17 at 10:03 PM UTC in A - Z Drug Synthesis

Ghost Black Hole

Originally posted by EllariaSand Lol

You’re a chemist now…..lol

Name the glassware in the video…in order

Explain the principle behind distillation…..layman’s terms

What are boiling chips and why are they added….not googled 🙄

Explain what a “base trap” is in layman’s terms…not googled…..

Thanks for ruining my thread bitch.

I'm on my phone but the synthesis of HI acid is done in a round bottom flask on heating mantle cranked up to max heat and the trap is to catch hydrogen sulfide.

Boiling chips are added to create nucleation points and you add them BEFORE the heat is cranked up or else everything goes sploosh

2018-06-17 at 9:24 PM UTC in A - Z Drug Synthesis

Ghost Black Hole

Starting from Toluene.

"o-Toluidine can be synthesized from toluene. The direct aromatic amination is very effective when done with a parent nitrenium ion, but o-toluidine can also be synthesized in other ways. For example, by the amination of toluene with methylhydroxylamine or hydroxylammonium salts in presence of aluminum trichloride"

https://pubs.acs.org/doi/abs/10.1021/j150226a002

Once you have o-Toluidine you can proceed to start making the precursor

http://www.prepchem.com/synthesis-of-2-methylbenzenediazonium/

"100 ml of concentrated hydrochloric acid (1.2 moles) and 50 ml of water are poured into a 500 ml flask. 43 grams (or 43 ml) of o-toluidine (0.4 mole) are added and well mixed in order to convert the o-toluidine into the o-toluidine hydrochloride. The solution is cooled with shaking in a salt-ice bath and the o-toluidine hydrochloride separates as fine crystals. By keeping the mixture at a temperature of 0-5° C and by vigorous shaking in the salt-ice bath the o-toluidine hydrochloride is treated with a solution of 28 grams of sodium nitrite in 80 ml of water with shaking. The o-toluidine hydrochloride dissolves as the more soluble 2-methylbenzenediazonium diazonium salt is formed, and at the end of the addition of the sodium nitrite the solution should contain a trace of nitrous acid. 2-methylbenzenediazonium is not stable and should be consumed."

Then you can make 2-chlorotoluene

"The solution of cuprous chloride is cooled in an ice bath 0-5° C temperature. In this cold solution, the 2-methylbenzenediazonium is poured with constant shaking and allowing the mixture to come to room temperature. After about 10 minutes, the mixture gradually warmed with a good shaking. As the temperature rises the brown addition product begins to decompose with the evolution of nitrogen and with the formation of an oily layer of 2-chlorotoluene. When the decomposition reaction is at an end, the mixture is steam distilled, continuing the process only as long as oily droplets are present in the distillate, for the product is not appreciably soluble in water. The layer of 2-chlorotoluene is carefully separated and washed twice with an equal volume of concentrated sulfuric acid, which removes both the 2-cresol and the azo compound. Then 2-chlorotoluene is washed with water in order to remove the inorganic acid. Finally, 2-chlorotoluene is dried over calcium chloride, distilled, using an air condenser and collecting the product boiling at 153-158° C. Pure 2-chlorotoluene boils at 157° C. The yield is 25-30 g."

Then you make 2-chlorobenzaldehyde

http://www.prepchem.com/synthesis-of-1-chloro-2-dichloromethylbenzene/

And then you can make 2-chlorobenzoyl chloride

https://patents.google.com/patent/US4388251

"The present application is directed to the preparation of 2-chlorobenzoyl chloride by the reaction of 2-chlorobenzaldehyde with chlorine in the presence of phosphorus pentachloride"

The synthesis is nearly finished now and we just have to form the benzodiazepine ring structure

https://erowid.org/archive/rhodium/chemistry/clonazepam.html

"3. Clonazepam (5-(2-chlorophenyl)-1,3-dihydro-7-nitrobenzo(1,4)-diazepin-2-one)
(see swiss patent 580,087, workup: US patent 3,335,181)

The 143 g (0.36 mol) intermediate from step 2, 101 g hexamethylenetetramine (urotropine) and 36 mL 99 % formic acid are suspended/dissolved in 5 L absolute ethanol, the mixture is refluxed with stirring for 4 h, and then the mixture is concentrated in vacuo to dryness. The residue is dissolved in 2 L dichloromethane and 4 L water, the organic layer is seperated and mixed with 2 L ethanol. Over a 20 cm vigreux column, the dicloromethane is distilled off and the residual solution is cooled to 0 C for 24 h. The almost yellow-white crystalls of Clonazepam are vacuum-enhancemented off and washed with 0 C ethanol, after drying, about 90.9 g (80%) of Clonazepam are resulting, mp. 235-237°C."

2018-06-17 at 9:10 PM UTC in Unban Infinityshock

Ghost Black Hole

Originally posted by aldra yeah that's what I mean, it's a permaban

temp bans are supposed to convince a user to change their behaviour, which absolutely doesn't work with him

His behavior is fine.

You are all just cucks.

2018-06-17 at 9:06 PM UTC in A - Z Drug Synthesis

Ghost Black Hole

B is for Benzodiazepine

2018-06-17 at 9:01 PM UTC in A - Z Drug Synthesis

Ghost Black Hole

An unlimited lifetime supply of ampetamine would not be very expensive to make.

Usually you just mix benzaldehyde and Nitroethane for p2np and reduce to amphetamine but Nitroethane has become very tightly controlled because of its use in MDMA manufacture and terrorism.

An alternate synthesis would be
to make p2p from MEK and benzaldehyde via Baeyer-Villiger oxidation and catalytically hydrogenate it to amphetamine.

You could make a kilogram for a few hundred dollars if you set it up properly.

Another way you could do this is get a bunch of Mandelic Acid (acne cream treatment, like Salicylic acid but stronger) and reduce it with HI acid (potassium iodide and phosphoric acid) to make phenylacetic acid to phenylacetone and then you do this

A mixture of 40 g (0.3 mole) phenylacetone, 200 ml ethanol, 200 ml 25% ammonia, 40g (1.5 mole) Al-grit and 0.3 g (1 mmol) HgCl2 is warmed with vigorous stirring until reaction takes place, after which warming is stopped immediately. Cooling should be applied if the reaction becomes too violent. When the violence of the reaction has diminished, the mixture is refluxed with vigorous stirring for about 2 hr, concentrated in vacuo to 200 ml and poured into ice water, alkalinized with 120 g KOH, and extracted with ether. The extractions are treated with 20% HCl, the resulting water layer alkalinized and extracted with 150 ml ether. The organic layer is dried over Na2SO4, the ether evaporated, and the residue distilled in vacuo. Yield: 12.5 g (30%).

Preparation of amphetamine sulfate yielded 96-98% product with a purity of 99.2-99.8% (USP grade).

Above reaction is nearly 100% OTC. Mandelic acid is not hard to get/make. HI acid is also pretty easy to make of you have the right glassware.

2018-06-17 at 9:01 PM UTC in A - Z Drug Synthesis

Ghost Black Hole

A is for Amphetamine

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