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A - Z Drug Synthesis
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2018-06-17 at 11:36 PM UTCI should be reporting you for being a pussy ass know nothing
You failed to address or mention the distillation tube……the single most crucial aspect of that process….moron
You were posting in other threads while I answered my own questions........
Keep crying ya pansy ass bitch boy.....I’m laughing my ass off -
2018-06-17 at 11:37 PM UTC
Originally posted by EllariaSand I should be reporting you for being a pussy ass know nothing
You failed to address or mention the distillation tube……the single most crucial aspect of that process….moron
You were posting in other threads while I answered my own questions……..
Keep crying ya pansy ass bitch boy…..I’m laughing my ass off
I'm not doing your homework for you, sorry.
you can shit post in this thread if you want though.
https://niggasin.space/thread/25533 -
2018-06-17 at 11:40 PM UTCFuck off moron
Originally posted by EllariaSand No dear…..boiling chips are added to inhibit boiling in the round bottom flask
Of course your “on the phone” lol
The distillation tube is used to collect the distillate at the proper temp…..as the different parts of the solution will evaporate at different temps
The red tubes introduce cool water into & out of the distillation tube to control the distillate collected
What you posted was said in the video
Love these pretend chemists
I’m surprised you can find your way to your mothers basement every night.....do you cry to her a lot? You poor little pussy -
2018-06-17 at 11:47 PM UTCProof making your own drugs with a grade 3 education doesn't work.
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2018-06-17 at 11:48 PM UTC
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2018-06-18 at 5:07 AM UTC
Originally posted by Ghost Reported for intentional disruption.
Enjoy your 2 week ban like your friend well-hung
"She is just posting the exact same stuff I posted and trying to disrupt my thread.
Please just delete the thread I can't stand to see all that hard work I put into my post ruined by some stupid bitch on her period"
Gotta be honesty here my dude, it looks like you're derailing this thread as much as anyone else is.
Ellaria has made a number of posts that seem technical and on-topic, and you don't seem to really be engaging with them seriously so much as saying "do your own homework" and complaining about her. The gif posting and name calling isn't appropriate for topical forums, I'll admit, but seeing as you've done more or less the same I'm not really inclined to do anything here.
Why don't you both discuss the topic without it devolving into a shitflinging contest? -
2018-06-18 at 5:46 AM UTCnigger
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2018-06-18 at 1:37 PM UTC
Originally posted by Lanny Gotta be honesty here my dude, it looks like you're derailing this thread as much as anyone else is.
Ellaria has made a number of posts that seem technical and on-topic, and you don't seem to really be engaging with them seriously so much as saying "do your own homework" and complaining about her. The gif posting and name calling isn't appropriate for topical forums, I'll admit, but seeing as you've done more or less the same I'm not really inclined to do anything here.
Why don't you both discuss the topic without it devolving into a shitflinging contest?
pls delete thread
Originally posted by apt Even if I hadn't taken enough chemistry classes in college to know OP is a charlatan, I still wouldn't take advice from someone whose greatest scientific accomplishment is blowing up his own house with a nigger-rigged meth lab
wasnt my fault. There just happened to be a meth lab in my house when it burned down that does not mean it burned the house down. Although the flammable chemicals didn't help, they were not the cause of the fire. -
2018-06-18 at 1:38 PM UTCOh quesrion about drugs: What is bundy or something like that u guys keep refering to?
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2018-06-18 at 1:43 PM UTC
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2018-06-18 at 1:50 PM UTC
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2020-07-06 at 1:08 AM UTC
Originally posted by Ghost Starting from Toluene.
"o-Toluidine can be synthesized from toluene. The direct aromatic amination is very effective when done with a parent nitrenium ion, but o-toluidine can also be synthesized in other ways. For example, by the amination of toluene with methylhydroxylamine or hydroxylammonium salts in presence of aluminum trichloride"
https://pubs.acs.org/doi/abs/10.1021/j150226a002
Once you have o-Toluidine you can proceed to start making the precursor
http://www.prepchem.com/synthesis-of-2-methylbenzenediazonium/
"100 ml of concentrated hydrochloric acid (1.2 moles) and 50 ml of water are poured into a 500 ml flask. 43 grams (or 43 ml) of o-toluidine (0.4 mole) are added and well mixed in order to convert the o-toluidine into the o-toluidine hydrochloride. The solution is cooled with shaking in a salt-ice bath and the o-toluidine hydrochloride separates as fine crystals. By keeping the mixture at a temperature of 0-5° C and by vigorous shaking in the salt-ice bath the o-toluidine hydrochloride is treated with a solution of 28 grams of sodium nitrite in 80 ml of water with shaking. The o-toluidine hydrochloride dissolves as the more soluble 2-methylbenzenediazonium diazonium salt is formed, and at the end of the addition of the sodium nitrite the solution should contain a trace of nitrous acid. 2-methylbenzenediazonium is not stable and should be consumed."
Then you can make 2-chlorotoluene
"The solution of cuprous chloride is cooled in an ice bath 0-5° C temperature. In this cold solution, the 2-methylbenzenediazonium is poured with constant shaking and allowing the mixture to come to room temperature. After about 10 minutes, the mixture gradually warmed with a good shaking. As the temperature rises the brown addition product begins to decompose with the evolution of nitrogen and with the formation of an oily layer of 2-chlorotoluene. When the decomposition reaction is at an end, the mixture is steam distilled, continuing the process only as long as oily droplets are present in the distillate, for the product is not appreciably soluble in water. The layer of 2-chlorotoluene is carefully separated and washed twice with an equal volume of concentrated sulfuric acid, which removes both the 2-cresol and the azo compound. Then 2-chlorotoluene is washed with water in order to remove the inorganic acid. Finally, 2-chlorotoluene is dried over calcium chloride, distilled, using an air condenser and collecting the product boiling at 153-158° C. Pure 2-chlorotoluene boils at 157° C. The yield is 25-30 g."
Then you make 2-chlorobenzaldehyde
http://www.prepchem.com/synthesis-of-1-chloro-2-dichloromethylbenzene/
And then you can make 2-chlorobenzoyl chloride
https://patents.google.com/patent/US4388251
"The present application is directed to the preparation of 2-chlorobenzoyl chloride by the reaction of 2-chlorobenzaldehyde with chlorine in the presence of phosphorus pentachloride"
The synthesis is nearly finished now and we just have to form the benzodiazepine ring structure
https://erowid.org/archive/rhodium/chemistry/clonazepam.html
"3. Clonazepam (5-(2-chlorophenyl)-1,3-dihydro-7-nitrobenzo(1,4)-diazepin-2-one)
(see swiss patent 580,087, workup: US patent 3,335,181)
The 143 g (0.36 mol) intermediate from step 2, 101 g hexamethylenetetramine (urotropine) and 36 mL 99 % formic acid are suspended/dissolved in 5 L absolute ethanol, the mixture is refluxed with stirring for 4 h, and then the mixture is concentrated in vacuo to dryness. The residue is dissolved in 2 L dichloromethane and 4 L water, the organic layer is seperated and mixed with 2 L ethanol. Over a 20 cm vigreux column, the dicloromethane is distilled off and the residual solution is cooled to 0 C for 24 h. The almost yellow-white crystalls of Clonazepam are vacuum-enhancemented off and washed with 0 C ethanol, after drying, about 90.9 g (80%) of Clonazepam are resulting, mp. 235-237°C."
bump -
2020-07-06 at 1:43 PM UTC
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2020-07-06 at 1:45 PM UTCP is for Pushing it to the limit
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2020-07-06 at 2:24 PM UTC
Originally posted by BeeReBuddy bump
I have no idea what this is. Starting from toluene is possible but uses some pretty hard to get things like chlorine gas and phosphorus pentachloride. The furthest back you could go for purchasing would be 2-chlorobenzaldehyde. I don't think anyone would expect someone is converting it to benzos.
This is more like a synthesis you would do if the world ended.
Originally posted by Kev ok we're at D so far? My turn?
E! Da love drug. If I saved the damn page JoePedo wrote on synthesizing it from vanillin extract, this post (and thread) would be gold.
Alas.
I'm familiar with the vanillin process. You can also get vanillin pretty easily in large amounts. I think they even sell it on eBay but some of the other things required are a bit tricky like phase transfer catalysts.
https://erowid.org/archive/rhodium/chemistry/methylenation.html -
2020-07-06 at 2:57 PM UTC
Originally posted by the man who put it in my hood I'm familiar with the vanillin process. You can also get vanillin pretty easily in large amounts. I think they even sell it on eBay but some of the other things required are a bit tricky like phase transfer catalysts.
https://erowid.org/archive/rhodium/chemistry/methylenation.html
Yeah thats the beauty of it, vanilla extract is super cheap. I think all the steps get you MDE (or MDA)? but a small final step is needed to get MDMA, i already forgot. would this be something someone completely chemistry-retarded like me could do? Joe's guide did say "home mdma production for the masses". -
2020-07-06 at 3:20 PM UTCSome of the chemicals needed are things that can be tricky to get. This was a lot more popular in the early 2000's when you could buy large amounts of precursors from a university account without raising much suspicion.
If you can source the reagents though it is totally within the possibility of a home chemist. You would have to have a full lab with a fume hood -
2020-07-06 at 5:04 PM UTChow do i make tylenol o'chosen one
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2020-07-06 at 5:17 PM UTC"Our new company is preparing to manufacture aspirin by synthesis from evergreen oil. The two step synthesis encompasses aqueous base hydrolysis of wintergreen oil (methyl salicylate, MS) to salicylic acid (SA) followed by acetylation to acetylsalicylic acid (aspirin, ASA)"
https://www.students2science.org/wp-content/uploads/2016/09/Salysylic_Acid_Synthesis_Instructor_Guide.pdf
You can also do it in reverse and make wintergreen oil from salicylic acid
