How do I make methyl iodide ? Methaylamine + iodine?
I made phenacealdehyde from phenylalanine I was thinking a methylgrinard reagent won’t convert to a intermediate that could be reduced to meth but I haven’t tried yet because I don’t know what Grignard reagent is best as there are many different versions
And methyl ethyl ketone is expesive is the any substitute or way to make it?
And yeah getting precursors from China what most do but making it from scratch is rare I couldn’t find any info on how to make it tho I even ask on Reddit and the say buy it
👍Good stuff where did you find the recipe for p2p ?
Get some pmk or Bmk acetate or gycidate they can be bought by the kilo and hydrolysis with hcl gives p2p in an oil layer separate oil with Coleman fuel and then refux with methylamine to get n methylformamide and then reduce with sodium borohydride to get n methyl amphetamine
2021-04-22 at 7:36 PM UTC
in
Shake and bake mephedrone
Is it cool if I refer people to this forum? I wasn’t sure if this forum was supposed to remain hidden or not so but I can tell people about this forum so we have more people also it’s easy to get ethyl phenylacetate or gylcidate then all you gotta do is hydrolysis with aqueous hcl to get a oil layer of p2p . Then just make methylamine with 40% formalin and amonium cloride
I exercise safety as well I use gas mask for organic vapors , wear flame resistant lab coat or overalls and built a homemade vapor hood with carbon enhancement and I try to always remember to wear gloves
So I gassed and had results this time but idk what the fuck I made it can’t be meth it burns and taste horrible. It could be because I didn’t clean the pills enough or maybe the ingredients they put in them nowadays but man I was looking forward to trying this because I wanted to experience what all the old Skool users call real d methamphetamine . I have only used the stuff that come from Mexico since 2017 which is not even close to the stuff made in the 1990s like lemon drop , peanut butter , lemon drop,and true glass shards . Idk what Mexico is be using to make the new stuff but from what I hear it’s not ephedrine . Since Mexico is the only source they take advantage buy cutting the shit out of dope I would not be suprised if they wipe they ass with the bricks before they sell to use just like the brown brick weed they used to supply America before we finally started to legalize dispensary and hood weed came about . I won’t quit tho I will find a way to bring back good meth and other substances . I have a theory that if I react bromoethylbezene with methlyamine it would produce ampetamine and they I would just have to do an indirect mono methylation but that’s a theory I have yet to try it mainly because I can’t find any info on it . I have found info on synthesis of 4 methylaminorex but the chemicals needed are hard to find . I’m also trying the oxidation of phenylalanine to phenlyacealdehye using sodium hypochlorite and sodium bicarbonate as ph buffer then potassium per magnet to further oxidize to phelylacetone then to methamphetamine grignarrd synthesis style but I’m learning chemistry on my own so I have trouble with some stuff but I got the basic idea and I always reading stuff on the internet to better understand .
I did try it with isopropyl as solvent the time before last reaction attempt but for some reason the bottle cracked on the botttom lucky it happens befor I put the pseudo in
Ammonium sulphate and sodium hydroxide with Coleman fuel as solvent . Is the solvent supposed to be completely clear when gassing? I think maybe I’m not shaking it enough . I’m trying it again right now this time I make sure to shake the shot out of it and I used less solvent so the concentration should be higher . I’m gonna gas with sulphuric acid on salt or is it better for aluminum and Muriatic acid?
No who’s enso and idk I have been letting the lithium get bronze and what not but when I gas the solvent nothing happens
Ok got it one more question when I gassing the solevent i can’t see any crystal forming? I completed reaction wait for solevent to clear up and then collected solevent and upon gassing no crystals formed idk what I’m doing wrong . I even washed solevent with water afterwards and then based the water with sodium carbonate to get meth back to feebase and extract with Coleman fuel and regassed and still nothing it must be a step or something I doing wrong
And doesn’t hcl+al —-> alcl + h2 ? Muriactic acid and aluminum make aluminum cliroide and hydrogen gas? How does it make hcl gas?
What is the best way to get solevent out of bottle when the still lithium floating on top ? I used too much lithium I think . I’m using real lithium metal not batteries.
Can dimethylphenethlyamine be mono unmethylated to methlyphenethlyamine?
Ok so I used a check back valve and now the liquid from the generator it be sucked into the sole vent . Also what is the reason every time I gas I don’t see 1 crystal form? I complet the reaction and have lost 6 pills boxes because I don’t know how to save the material after it’s been contaminated should I post pics
I seem to have make the achocol as the product smelled like an alcohol I put phenylalanine into a jar with distill water. Then I added sodium borohydire and mix and left in the sun to warm up . Then a half a day later I put isopropyl mixed with methanol into the reaction jar. I let us sit so an hour or so the I straind with coffee enhancement and then the cloudy liquid I used Coleman camp fuel to extract. When the water looke clearer and the Coleman fuel cloudy I separated the 2 liquid and set out to dry.I hoping it’s not gonna rain today but if it does then it will delay the dry time.
I want to try this reaction phenylalanine to pheylniniol using sodium botohydride I found stuff on internet saying it would work but then from the alcohol I want to reduce methlyphenethlyamine or oxidize Ketone using potassium permaganye witch route is best you think?
Ok I will get one .do you know what the most efficient and clean way to obtain pure pseudoephedrine from ephedra? I be using rubbing alcohol but it extracts a lot of chlorophyll and other stuff from plant . I think pseudoephedrine is a freebase when in plant so not sure if it water soluble. It is made into tea tho so maybe it is but wouldn’t heat destroy the alkaloids?
