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Shake and bake mephedrone

  1. #1
    Ghost Black Hole
    "DEBK" is Russian for 4-methylbromopropiophenone. Get some of that and make methylamine from hexamine and you can do this reaction at home

  2. #2
    gadzooks Dark Matter [keratinize my mild-tasting blossoming]
    I think I tried mephedrone once... I'm not 100% sure what it was... It was almost 10 years ago. I bought it online. It was some kind of stimulant, but it was not meth or coke. It almost certainly started with M (but so do lots of stimulants).

    I remember it being not too bad, whatever it was. I'm not super into stimulants, though. But I am curious to try it again.
  3. #3
    gadzooks Dark Matter [keratinize my mild-tasting blossoming]
    You know what, i may be thinking of 4-FA... I found an old record from about that time period where I mentioned doing 4-FA.

    I guess I don't know mephedrone.

    Heck, I don't even really know much about 4-FA, but apparently I've tried it.
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  4. #4
    gadzooks Dark Matter [keratinize my mild-tasting blossoming]
    Omg mephedrone is related to MCAT...

    That's why it sounds familiar!

    I've never done it, but like 15 years ago I was research how to synthesize it (methcathinone) because it looked easier than meth would have been.
  5. #5
    Ghost Black Hole
    Yeah it's made like meth starting with sudafed but instead of red phosphorus/iodine you use potassium permanganate

    I haven't tried mephedrone or any analogs yet :(
  6. #6
    Grylls Cum Looking Faggot [abrade this vocal tread-softly]
    taht looks danerous
  7. #7
    Ghost Black Hole
    how to make methylamine from hexamine



    and here is a source for the main feedstock precursor. I don't know how to make it yet but I will keep looking

  8. #8
    Ghost Black Hole
    okay I figured it out:

    http://www.namsdl.org/library/E322C098-1372-636C-DD4851FCC1E15FB7/

    "As for other ring-substituted N-methylcathinone derivatives, the most likely and straightforward route of synthesis for mephedrone is by reacting the suitably substituted bromopropiophenone with methylamine; the resulting product is always racemic. Therefore, mephedrone is most likely synthesised by bromination of 4-methylpropiophenone (1-(4-methylphenyl)-1-propanone) followed by reaction of the resulting 4-methylbromopropiophenone (1-(4-methylphenyl)-2-bromo-1-propanone) with an excess of methylamine or methylamine hydrochloride and an acid scavenger. The reaction is then quenched with gaseous or aqueous hydrochloride providing the hydrochloride salt that should be recrystallised. This is one of the simplest choices because the starting materials are often commercially available or easily synthesised. This requires similar equipment and chemical knowledge to that needed for the synthesis of e.g. amphetamine or MDMA"

    How to make 4-methylpropiophenone

    https://the-hive.archive.erowid.org/forum/showflat.pl?static=1&Cat=&Number=423945
    https://thosci.com/synthesis-of-4-methylpropiophenone/

    To a reflux apparatus add 100 mL of dry toluene and 47 g of anhydrous aluminum trichloride, with vigorous stirring, add 25 mL of propionyl chloride, after the addition, heat the mixture under reflux for 2h. After the reflux, the mixture is poured into 100 g of ice with 30 mL of conc. HCl, the organic phase is washed with 40 mL of water, 2×20 mL of dilute NaOH and 4×40 mL of water, the organic layer is dried over anhydrous calcium chloride and it is distilled with collecting the fraction of 230-236°C.



    Addition of the propionyl chloride and refluxing for 2h



    The distilled 4-methylpropiophenone

    '

    not exactly OTC but it's a start. Next I will post how to make propionyl chloride.
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  9. #9
    gadzooks Dark Matter [keratinize my mild-tasting blossoming]
    Man, this thread really single handedly my proves why we need more members posting here.

    I'm working on that, via a couple different angles, but most people don't seem all that concerned.

    The thing is, that would result in more people that might be willing to engage in discussion and... Might even bring a certain degree of expertise/knowledge/ideas to the table.

    Threads like this just end up with the two of us, and then ultimately you just end up finding a solution on your own.

    We need to establish a space that fosters more contribution and more back and forth.

    I'm working on my Chem knowledge as best I can so I can be of more help, but more people would help too.
  10. #10
    ECAP Tuskegee Airman
    The following users say it would be alright if the author of this post didn't die in a fire!
  11. #11
    Bologna Nacho African Astronaut
    I am at steak n shake
  12. #12
    Grylls Cum Looking Faggot [abrade this vocal tread-softly]
    i am eating a steak bake
  13. #13
    gadzooks Dark Matter [keratinize my mild-tasting blossoming]
    Originally posted by ECAP

    The batteries are an awesome touch.
  14. #14
    ECAP Tuskegee Airman
    Originally posted by gadzooks The batteries are an awesome touch.

    Right!! Capital
    L
    O
    L
  15. #15
    jessetovar420 Yung Blood [excrete my arguable empowerment]
    Is it cool if I refer people to this forum? I wasn’t sure if this forum was supposed to remain hidden or not so but I can tell people about this forum so we have more people also it’s easy to get ethyl phenylacetate or gylcidate then all you gotta do is hydrolysis with aqueous hcl to get a oil layer of p2p . Then just make methylamine with 40% formalin and amonium cloride
  16. #16
    Ghost Black Hole
    fuck the video got removed
  17. #17
    Bradley African Astronaut
    Originally posted by gadzooks The batteries are an awesome touch.

    they're the wrong type.
  18. #18
    Bradley African Astronaut
    Originally posted by jessetovar420 Is it cool if I refer people to this forum? I wasn’t sure if this forum was supposed to remain hidden or not so but I can tell people about this forum so we have more people also it’s easy to get ethyl phenylacetate or gylcidate then all you gotta do is hydrolysis with aqueous hcl to get a oil layer of p2p . Then just make methylamine with 40% formalin and amonium cloride

    yes refer everyone especially ppl you know irl
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