synmeg synthetic nutmeg

1. 2016-02-06 at 2:29 AM UTC

   #1
   The Self Taught Man Black Hole
   Abstract: The synthesis of myristicin ketone from myristicin has been achieved through conversion of allyl group to ketone. Myristicin was isolated from nutmeg oil. The reaction of myristicin with mercury acetate in aqueous tetrahydrofuran, followed by in situ reduction of the mercurial intermediate by alkaline solution sodium borohydride produced myristicin alcohol. Myristicin alcohol was oxidized with PCC at 40 0C for 90 minutes, followed by purified with saturated potassium disulphite yield myristicin ketone (3-methoxy-4,5-methylenedioxyphenyl)-2-propanone (68.32%).
2. 2016-02-06 at 10:18 AM UTC

   #2
   The Self Taught Man Black Hole
   dude...make the first line of nutmeg-based RCs
3. 2016-02-07 at 7:14 AM UTC

   #3
   

   Dissociator African Astronaut
   ^^^^^###^^^^^ ^^^"":;;:""^^^ O_oooooooo It's a monster
4. 2016-02-07 at 1:48 PM UTC

   #4
   The Self Taught Man Black Hole

   dude…make the first line of nutmeg-based RCs

   
   
   Sploo labs needs more ideas
5. 2017-04-02 at 9:24 AM UTC

   #5
   The Self Taught Man Black Hole

   Originally posted by SCronaldo_J_Trump Abstract: The synthesis of myristicin ketone from myristicin has been achieved through conversion of allyl group to ketone. Myristicin was isolated from nutmeg oil. The reaction of myristicin with mercury acetate in aqueous tetrahydrofuran, followed by in situ reduction of the mercurial intermediate by alkaline solution sodium borohydride produced myristicin alcohol. Myristicin alcohol was oxidized with PCC at 40 0C for 90 minutes, followed by purified with saturated potassium disulphite yield myristicin ketone (3-methoxy-4,5-methylenedioxyphenyl)-2-propanone (68.32%).